Hydrochloric Acid → HCID 67695326, compound

HRID 1599961Notes

Reaction equation

HRID 1599961 reaction equation
[NH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[C:8]([CH2:11][CH2:12][C:13]3[CH:23]=[CH:22][C:16]([C:17]([O:19]CC)=[O:18])=[CH:15][CH:14]=3)[N:9]=2)[CH2:4][CH2:3][CH2:2]1.[ClH:24]>>[ClH:24].[NH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[C:8]([CH2:11][CH2:12][C:13]3[CH:14]=[CH:15][C:16]([C:17]([OH:19])=[O:18])=[CH:22][CH:23]=3)[N:9]=2)[CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 18928539HCID 18928539, compound

Product 1

HCID 67695326HCID 67695326, compound

Procedure

Ester 37-5 (680 mg, 2.11 mmol) in 10 mL 6N HCl was heated to 50° C. for 18 hours. Concentration provided 34-7 as a yellow solid.

Workup

  1. concentrationConcentration

Sources & evidence

ORD record
ord-5a4c90d6181c4d2fb860f986448d9cdf
Source dataset
uspto-grants-1998_04
Patent number
US05741796

Reaction notes

Loading…