HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → HCID 15672345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | HCID 15672343 | HCID 15672343 | — |
| Product | HCID 15672345 | HCID 15672345 | — |
Reaction Steps
Analogously to Example 8, 35 g (114 mmol) of 3-(2,4-dichloro-5-methylphenyl)-5-difluoromethoxy-1-methyl-1H-pyrazole were reacted with 16.9 g (125 mmol) of sulfuryl chloride. Yield: 30.8 g; 1H-NMR (270 MHz, in CDCl3): δ [ppm]=7.49 (s,1H), 7.30 (s,1H), 6.74 (t,1H), 3.85 (s,3H), 2.39 (s,3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744426 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-5f7cb530ec94455692977c5284e8b4f1 |
| Source note | uspto-grants-1998_04 |