Hydrochloric Acid → HCID 19365553, compound

Participants

Reaction Steps

The compound (0.54 g, 0.87 mmol) obtained in Example 19 and iron powder (0.26 g, 4.3 mmol) were added to methanol (10 ml) and to the mixture conc.hydrogen chloride (5 ml) was added dropwise for one hour. The mixture was stirred for 5 hours under ice-cooling. To the reaction mixture saturated sodium bicarbonate (30 ml) was added carefully. After adding chloroform (50 ml) and Celite, the mixture was subjected to filtration.

Provenance & Evidence