HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 22869819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Potassium ethanethioate | HCID 23670855 | — |
| Reactant | HCID 131720629 | HCID 131720629 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 22869819 | HCID 22869819 | — |
Reaction Steps
The title compound is prepared by the procedure of Example 111 using 2.22 gof product from Example 116, 1.01 g of potassium thioacetate and 25 ml of acetonitrile to give 0.90 g of the desired product after chromatography (silica gel: 30% ethyl acetate/hexane). IR(neat): 2100 and 1692 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744465 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-0aacd31026024d6f814d2fdd24fdfb06 |
| Source note | uspto-grants-1998_04 |