HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → Diisopropylethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Ethyl acetate hexane | HCID 21226206 | — |
| Reactant | HCID 22869819 | HCID 22869819 | — |
| Product | Diisopropylethylamine | HCID 81531 | — |
Reaction Steps
The title compound is prepared by the procedure of Example 17 using 0.441 gof product from Example 118 in 10 ml of acetonitrile, 1.8 g of product fromExample 15 in 10 ml of acetonitrile and 0.41 ml of Hunig's base to give 0.747 g of the desired product after chromatography (silica gel: 75% ethylacetate/hexane). IR(KBr): 2101, 1769 and 1708 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744465 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-ab56ba29d40b483da136cd9acdd9c1d3 |
| Source note | uspto-grants-1998_04 |