HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 18923982, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Anisole | HCID 7519 | — |
| Reactant | HCID 67707349 | HCID 67707349 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 18923982 | HCID 18923982 | 86.9% |
Reaction Steps
The title compound is prepared by the procedure of Example 202 using 0.615 g of product from Example 177, 1.04 g of mercuric trifluoroacetate, 0.440 g of anisole and 31 ml of 80% acetic acid to give, after chromatography (Silica gel: 10-100% ethyl acetate/hexane), 0.322 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744465 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-72bd509072b8410d84e0f8fe1f034498 |
| Source note | uspto-grants-1998_04 |