HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 18926605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | N,N-Dimethyl-1-(2-methyl-5-nitro-1H-indol-3-yl)methanamine | HCID 280316 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 18926605 | HCID 18926605 | 89.4% |
Reaction Steps
Treatment of 2, N,N-trimethyl-5-nitro-1H-indole-3-methanamine (J.Org.Chem.,28,2921(1963)) (5.60 g) with imidazole (1.90 g) in xylene (100 ml) according to the method of Preparation 1 gave the title compound (5.50 g),m.p. 240°-242° C. Found: C,61.02; H,4.41; N,21.68. C13 H12N4O2 requires: C,60.92; H,4.72; N,21.87%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744488 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-d93916c46aef4da4bb5ce4f36aee5c77 |
| Source note | uspto-grants-1998_04 |