HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium formate → HCID 18926515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium formate | HCID 2723923 | — |
| Reactant | HCID 86752489 | HCID 86752489 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 18926515 | HCID 18926515 | 90.2% |
Reaction Steps
Treatment of t-butyl (E)-3-[1-(2-methoxycarbonylethyl)-3-(3-pyridylmethyl)-1H-indole-4-yl]-2-propenoate (5.15 g) with 10% palladium on carbon (0.50 g) and ammonium formate (7.71 g) according to the method of Preparation 23 gave the title compound, (4.67 g) m.p. 80°-82° C. Found: C,71.43; H,7.06; N,6.35. C25H30N2O4 requires: C,71.06; H,7.16; N,6.63%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744488 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-fef2ecb9e9f24eb785afb905bb9f56e2 |
| Source note | uspto-grants-1998_04 |