HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 18939128, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 18926705 | HCID 18926705 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 18939128 | HCID 18939128 | — |
Reaction Steps
75.0 g of 25% strength ammonia are added dropwise with stirring to 25.2 g (0.1 mol) of methyl 4-(2-hydroxy-2-methylpropionyl)phenoxyacetate (obtained by esterifying compound IIg using methanol) in 50 ml of dioxane.After being stirred for 2 hours, the mixture is evaporated to solidification. The crude product is recrystallized from hot water, 22.1 gof compound IIt of melting point 139° C. being obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744512 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-839d99c2d7cf4887b20f30dc4c12c7cb |
| Source note | uspto-grants-1998_04 |