HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3-(3-Cyclopropylmethoxy-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3-(3-Cyclopropylmethoxy-1,2,5-thiadiazol-4-yl)pyridine | HCID 19075239 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-(3-Cyclopropylmethoxy-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide | HCID 19075467 | — |
Reaction Steps
A mixture of methyl iodide (0.25 ml, 4 mmol) and 3-(3-cyclopropylmethoxy-1,2,5-thiadiazol-4-yl)pyridine (400 mg, 1.7 mmol) in acetone (5 ml) was stirred at room temperature for 36 h. The title compound precipitated from the solution and was collected by filtration toyield 0.41 g (65%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744489 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-11b638351e8a40ff925f24e252e958cf |
| Source note | uspto-grants-1998_04 |