HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3-(3-(4-Methylpiperidino)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3-(3-(4-Methylpiperidino)-1,2,5-thiadiazol-4-yl)pyridine | HCID 19075317 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-(3-(4-Methylpiperidino)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide | HCID 19075375 | — |
Reaction Steps
A mixture of methyl iodide (0.5 ml, 8 mmol) and 3-(3-(4-methylpiperidino)-1,2,5-thiadiazol-4-yl)pyridine (0.8 g, 3.1 mmol)in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration toyield 1.14 g (92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744489 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-4fec0d57ff54434abec49ae355140ef6 |
| Source note | uspto-grants-1998_04 |