HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 18927150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Guanidine | HCID 3520 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-chloro-2-methyl-5-(methylsulfonyl)Benzoic acid | HCID 10824478 | — |
| Reactant | 2-Methyl-4-methylsulfinyl-5-methylsulfonylbenzoyl chloride | HCID 18927431 | — |
| Product | HCID 18927150 | HCID 18927150 | — |
Reaction Steps
Analogously to Example 1, by reaction of 1.3 g of 2-methyl-4-methylsulfinyl-5-methylsulfonylbenzoyl chloride [obtainable by reaction of 2-methyl-4-chloro-5-methylsulfonylbenzoic acid with Na methanethiolate, subsequent partial oxidation with hydrogen peroxide and conversion into the acid chloride, e.g. with SOCl2 ] with guanidine, N-diaminomethylene-2-methyl-4-methylsulfinyl-5-methylsulfonylbenzamide is obtained after customary working up and recrystallization from diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05744641 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-baddab8ef7bc48369dc82d6de3f56439 |
| Source note | uspto-grants-1998_04 |