Ethyl vinyl ether → HCID 131721424, compound

HRID 1600502Notes

Reaction equation

HRID 1600502 reaction equation
[OH:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[CH2:7])=[CH:4][CH:3]=1.[C:10](#[N:15])/[CH:11]=[CH:12]/[C:13]#[N:14].[CH2:16]([O:18][CH:19]=[CH2:20])[CH3:17]>>[CH2:16]([O:18][CH2:19][CH2:20][O:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[CH2:7])=[CH:4][CH:3]=1)[CH3:17].[OH:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[CH2:7])=[CH:4][CH:3]=1.[C:10](#[N:15])/[CH:11]=[CH:12]/[C:13]#[N:14]

Participants

3

Reactant 2

HCID 8023Ethyl vinyl etherHCID 86754728HCID 86754728, compound

Product 1

HCID 131721424HCID 131721424, compound

Procedure

Using 9.0 g of poly(p-hydroxystyrene/fumaronitrile) obtained according to (2) above and 2.8 g of ethylvinyl ether, the procedure of (3) of Preparation Example 1 was carried out for reaction and after-treatments to obtain 8.3 g of poly(p-1-ethoxyethoxystyrene/p-hydroxystyrene/fumaronitrile) as white powdery crystal. P-1-ethoxyethoxystyrene unit/p-hydroxystyrene unit molar ratio in the polymer≈3:7 (1H NMR). Mw≈20,000; Mw/Mn=1.85 (GPC with polystyrene calibration).

Workup

  1. customobtained
  2. customwas carried out for reaction

Sources & evidence

ORD record
ord-5c188b70ae864d0fab4df9ba357e6c7a
Source dataset
uspto-grants-1999_11
Patent number
US05976759

Reaction notes

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