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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1600529Generated: October 28, 2026

Sodium Hydroxide → HCID 21829895, compound

https://huagongshe.com/reaction/1600529

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium HydroxideHCID 14798—
ReactantHCID 15456866HCID 15456866—
SolventEthanolHCID 702—
ProductHCID 21829895HCID 2182989574.7%

Reaction Steps

To a solution of methyl 2-methyl-2-(6-methyl-5-phenyl-2, 3-dihydro-4-oxo-4 H-1,3-oxazin-3-yl)-butyrate (1.91 g) in 20 ml of ethanol was added at room temperature 30 ml of aq. NaOH (0.3N). After stirring for 24 h, ethanol was evaporated, and the mixture was acidified by hydrochloric acid. The precipitate was filtered off and dried to get the captioned compound (1.36 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05977025
Source datasetuspto-grants-1999_11
ORD IDord-fd3446a511444dd896718be1ca87c5f1
Source noteuspto-grants-1999_11