HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 21829895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 15456866 | HCID 15456866 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21829895 | HCID 21829895 | 74.7% |
Reaction Steps
To a solution of methyl 2-methyl-2-(6-methyl-5-phenyl-2, 3-dihydro-4-oxo-4 H-1,3-oxazin-3-yl)-butyrate (1.91 g) in 20 ml of ethanol was added at room temperature 30 ml of aq. NaOH (0.3N). After stirring for 24 h, ethanol was evaporated, and the mixture was acidified by hydrochloric acid. The precipitate was filtered off and dried to get the captioned compound (1.36 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977025 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-fd3446a511444dd896718be1ca87c5f1 |
| Source note | uspto-grants-1999_11 |