Hydrochloric Acid → HCID 67575744, compound

HRID 1600659Notes

Reaction equation

HRID 1600659 reaction equation
[CH3:1][N:2]1[C:7](=[O:8])[CH:6]=[N:5][N:4]([CH2:9][CH2:10][CH2:11][CH2:12][N:13]2[CH2:18][CH2:17][N:16]([C:19]3[CH:24]=[CH:23][CH:22]=[C:21]([Cl:25])[CH:20]=3)[CH2:15][CH2:14]2)[C:3]1=[O:26].Cl>C(O)C>[ClH:25].[CH3:1][N:2]1[C:7](=[O:8])[CH:6]=[N:5][N:4]([CH2:9][CH2:10][CH2:11][CH2:12][N:13]2[CH2:18][CH2:17][N:16]([C:19]3[CH:24]=[CH:23][CH:22]=[C:21]([Cl:25])[CH:20]=3)[CH2:15][CH2:14]2)[C:3]1=[O:26]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 21830772HCID 21830772, compound

Product 1

HCID 67575744HCID 67575744, compoundYield 195.5%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent2×

Procedure

The compound 4 (2.5 g) is taken up in ethanol (50 ml) and supplemented with a saturated hydrochloric acid solution in ethanol. After filtration, the precipitate is impasted in boiling ethanol (50 ml), drained, washed with ethyl ether and dried under vacuum at 80° C. to give 5 (2.68 g).

Workup

  1. filtrationAfter filtration
  2. washwashed with ethyl ether
  3. customdried under vacuum at 80° C.

Sources & evidence

ORD record
ord-f52ea0453cab49eabab463668ed3b6e6
Source dataset
uspto-grants-1999_11
Patent number
US05977106

Reaction notes

Loading…