HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → 1-(Phenylsulfanyl)-4-pyridin-3-ylbutan-2-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 10877288 | HCID 10877288 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1-(Phenylsulfanyl)-4-pyridin-3-ylbutan-2-ol | HCID 22465339 | 76.7% |
Reaction Steps
Prepared according to the method described in Example 1a) from thiophenol (0.142 g), sodium hydride (0.062 g) and 3-(2-oxiranylethyl)pyridine (0.150 g) in dimethylformamide at room temperature to give the title compound as an oil (0.200 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977105 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-f85d8bb5ed7f4a6e81fecacf33db5f8f |
| Source note | uspto-grants-1999_11 |