참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Boron tribromide | HCID 25134 | — |
| 반응물 | 2-(4-Methoxy-phenyl)-thiazole | HCID 11298449 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 4-(1,3-Thiazol-2-yl)phenol | HCID 223840 | — |
반응 단계
Prepared according to the method described in Example 36b) from 2-(4-methoxyphenyl)thiazole (1.7 g), dichloromethane (20 ml) and boron tribromide (1.0 M in dichloromethane, 17.8 ml) with stirring at -78° C. After work up the residue was triturated with ether to give the sub-title compound a pale yellow solid (1.2 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05977105 |
|---|
| 출처 데이터셋 | uspto-grants-1999_11 |
|---|
| ORD ID | ord-8619ce348643452fb449d8cd8f67af90 |
|---|
| 출처 메모 | uspto-grants-1999_11 |
|---|
