HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzophenone → HCID 21830698, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzophenone | HCID 14347 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 22465338 | HCID 22465338 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21830698 | HCID 21830698 | 21.4% |
Reaction Steps
Prepared according to the method described in Example 24b) from (±)-α-(chloromethyl)-3-pyridinepropanol (1.05 g), 4-hydroxybenzophenone (1.35 g), ethanol (30 ml) and aqueous sodium hydroxide (1.4 M, 5 ml). After work up the residue was purified by column chromatography over silica with ether then ethyl acetate to give the title compound as an oil (0.42 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977105 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-cf7a482de135439c827cb460735e48a4 |
| Source note | uspto-grants-1999_11 |