Sodium borohydride → HCID 15885181, compound

Participants

Reaction Steps

The imine from Step 2 was dissolved in absolute EtOH (25 mL) and NaBH4 (0.303 g, 8.0 mmol) was added. After 2 h, the solvent was removed and the residue treated with 1N HCL. Conc. NH40H was added to the solution which was then extracted with CH2Cl2 (3×), washed with brine, dried and concentrated to give the title compound as a viscous oil which was used as such.

Provenance & Evidence