Hydrochloric Acid → HCID 178499561, compound

HRID 1601042Notes

Reaction equation

HRID 1601042 reaction equation
[ClH:1].[NH:2]1[CH:6]=[C:5]([CH2:7][C:8]([OH:10])=[O:9])[N:4]=[CH:3]1.Cl.[CH3:12]O>>[ClH:1].[CH3:12][O:9][C:8](=[O:10])[CH2:7][C:5]1[N:4]=[CH:3][NH:2][CH:6]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 178479752HCID 178479752, compound

Product 1

HCID 178499561HCID 178499561, compound

Procedure

A solution of 1H-imidazole-4-acetic acid hydrochloride (4.00 g, 24.6 mmol) in methanol (100 mL) was saturated with gaseous hydrogen chloride. The resulting solution was allowed to stand at room temperature for 18 h. The solvent was evaporated in vacuo to afford the title compound as a white solid.

Workup

  1. customThe solvent was evaporated in vacuo

Sources & evidence

ORD record
ord-ccf66c8d654944d2adb6c383289518c9
Source dataset
uspto-grants-1999_11
Patent number
US05977134

Reaction notes

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