HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 86754743, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 86754744 | HCID 86754744 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Sodium Chloride | HCID 5234 | — |
| Product | HCID 86754743 | HCID 86754743 | — |
Reaction Steps
1 g of the product obtained in Stage A above is introduced into 50 cm3 of dioxane and 5 cm3 of concentrated sulphuric acid is added. The solution is heated for about 5 hours, diluted with water, saturated with NaCl and extraction is carried out with CHCl3 with 20% MeOH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977155 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-8bca80b0445a4a77afdd7cf8d0022cb6 |
| Source note | uspto-grants-1999_11 |