HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 6-(2,2,3,3-tetrafluoropropoxy)nicotinate → [6-(2,2,3,3-Tetrafluoropropoxy)pyridin-3-yl]methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 6-(2,2,3,3-tetrafluoropropoxy)nicotinate | HCID 18363323 | — |
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Product | [6-(2,2,3,3-Tetrafluoropropoxy)pyridin-3-yl]methanol | HCID 18363303 | 100% |
Reaction Steps
Ethyl 6-(2,2,3,3-tetrafluoropropoxy)nicotinate was reduced with diisobutyl aluminum hydride in the same manner as in Reference example 21 to obtain the title compound as an oil in a yield of 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05977152 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-7a07edd84fc148859b3ded99d171ad2f |
| Source note | uspto-grants-1999_11 |