Hydrochloric Acid → HCID 15869768, compound

Participants

Reaction Steps

A mixed solution of 1-(4-trifluoromethylphenyl)-5-(2-chloro-4-trifluoromethyl-N-methoxycarbonyl-anilino)tetrazole (1.2 g), methanol (15 ml) and potassium hydroxide (0.4 g) was stirred at room temperature for 3 hours. After the completion of the reaction, hydrochloric acid (5%; 80 ml) was added thereto. The precipitated crystals were collected by filtration and washed with water to obtain 1-(4-trifluoromethylphenyl)-5-(2-chloro-4-trifluoromethylanilino)tetrazole (1.0 g).

Provenance & Evidence