HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Nitroveratraldehyde → HCID 53763953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Nitroveratraldehyde | HCID 88505 | — |
| Reactant | 5,6-dimethoxy-3,4-dihydro-1H-naphthalen-2-one | HCID 4610752 | — |
| Product | HCID 53763953 | HCID 53763953 | — |
Reaction Steps
Prepared from 5,6-dimethoxy-2-tetralone and 2-nitro-4,5-dimethoxybenzaldehyde; mp 70-72° C.; IR (Nujol): 1715, 1550; 1H NMR: δ2.59 (2H, t), 3.06 (2H, t), 3.78 (3H, s), 3.86 (3H, s), 3.88 (3H, s), 3.92 (3H, s), 6.47 (1H, s), 6.77 (1H, d, J=8.2), 7.41 (1H, d, J=8.2), 7.67 (1H, s); 13C NMR: δ19.7, 32.0, 56.3, 56.7, 56.8, 56.85, 108.1, 121.9, 125.6, 126.1, 128.0, 129.2, 132.1, 132.9, 133.7, 140.3, 141.4, 149.3, 152.9, 153.5, 200.9; Anal. (C21H21NO7) C, H, N.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981541 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-4923bde092fc452fa43f16a08b78dee6 |
| Source note | uspto-grants-1999_11 |