HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178479206, compound → Ammonia
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178479206 | HCID 178479206 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Ammonia | HCID 222 | — |
| Product | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178510920 | HCID 178510920 | — |
Reaction Steps
There is obtained from 4-(4-[2-cyano-ethyl]-phenylamino)-3-phenylamino-1H-pyrazolo[3,4-d]pyrimidine (see Example 7), by reduction with Raney nickel in a solution of ammonia in methanol and subsequent treatment with hydrogen chloride in ethanol, 4-(4-[3-amino-propyl]-phenylamino)-3-phenylamino-1H-pyrazolo[3,4-d]pyrimidine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981533 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-f304ea0f9de24fed82e15c28777643ab |
| Source note | uspto-grants-1999_11 |