HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloroaniline → Benzenamine, 3-chloro-, hydrochloride (1:1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Benzenamine, 3-chloro-, hydrochloride (1:1) | HCID 67336 | — |
Reaction Steps
60 g (0.47 mol) of 3-chloro-aniline are dissolved in 255 ml (0.56 mol) of a 2.2N solution of HCl in methanol. Concentration and stirring of the residue in diethyl ether, followed by filtering and drying, yield 3-chloro-aniline hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981533 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-716cca8cf89f4b078fd6676e238ea6d7 |
| Source note | uspto-grants-1999_11 |