HRID1602227

反应详情

EQUATION

反应方程式

HRID 1602227 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

60 g (0.47 mol) of 3-chloro-aniline are dissolved in 255 ml (0.56 mol) of a 2.2N solution of HCl in methanol. Concentration and stirring of the residue in diethyl ether, followed by filtering and drying, yield 3-chloro-aniline hydrochloride.

WORKUP

后处理

  1. concentrationConcentration
  2. filtrationby filtering
  3. customdrying