HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 19610575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-Methoxybenzylamine | HCID 75452 | — |
| Reactant | 2-(Bis(methylsulfanyl)methylidene)propanedinitrile | HCID 99229 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 19610575 | HCID 19610575 | — |
Reaction Steps
A mixture of 17.03 g (0.1 mol) of 3,3-bis-methylmercapto-2-cyano-acrylonitrile, 12.98 ml (0.1 mol) of 4-methoxy-benzylamine and 60 ml of ethanol is heated under reflux for 2 hours. Approx. 90 ml of hexane are then added dropwise to the hot solution which is then allowed to cool to RT. The title compound which has precipitated in the form of colorless crystals is filtered off, washed with diethyl ether and dried under a HV; m.p. 100-101° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981533 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-4c89c6156c834c649b6a0d3f7b08071c |
| Source note | uspto-grants-1999_11 |