HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15663660, compound → HCID 19610888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15663660 | HCID 15663660 | — |
| Reactant | HCID 178419492 | HCID 178419492 | — |
| Product | HCID 19610888 | HCID 19610888 | 56% |
Reaction Steps
5-(Tetrazol-2-yl)-1-azabicyclo[3.2.1]octane (the free base of E29) (0.2 g, 1.12 mmol) was converted to the 5-bromotetrazole according to the method of Example 40. Chromatography on silica using 4% methanol/chloroform afforded the title compound (E50) as a white crystalline solid (0.16 g, 56%) m.p. 108-110° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981545 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-9817e9d877504814a86c60f55debf3e8 |
| Source note | uspto-grants-1999_11 |