Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Formate | HCID 2735122 | — |
| Reactant | 4,5-Bis(bromomethyl)-1,3-dioxol-2-one | HCID 12325849 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19611269 | HCID 19611269 | 65% |
Reaction Steps
4,5-Dibromomethyl-2-oxo-1,3-dioxolene (150 mg, 0.55 mmol) was dissolved in acetonitrile (4.0 mL). Potassium formate (46 mg, 0.55 mmol) was added thereto. This mixture was stirred at 25° C. for 5 hours. Through the ordinary post-treatment, crude Compound S-30 (85 mg, yield 65%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05981558 |
|---|
| Source dataset | uspto-grants-1999_11 |
|---|
| ORD ID | ord-d8e99cc22ae9474396133de3b0e872aa |
|---|
| Source note | uspto-grants-1999_11 |
|---|
