Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 19611268 | HCID 19611268 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 19611273 | HCID 19611273 | 95% |
Reaction Steps
4-Acetoxymethyl-5-methyl-2-oxo-1,3-dioxolene (159 mg, 0.92 mmol) was dissolved in carbon tetrachloride (5.0 mL). Thereto were added N-bromosuccinimide (164 mg, 0.92 mmol) and benzoyl peroxide (11 mg, 0.046 mmol). This mixture was stirred at 80° C. for 1 hours. Through the ordinary post-treatment, crude Compound S-31 (220 mg, yield 95%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05981558 |
|---|
| Source dataset | uspto-grants-1999_11 |
|---|
| ORD ID | ord-f072fe8a07954f2ab587aaff355ce561 |
|---|
| Source note | uspto-grants-1999_11 |
|---|
