HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 12661867, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 19611657 | HCID 19611657 | — |
| Reactant | HCID 19611693 | HCID 19611693 | — |
| Catalyst | Benzoyl Peroxide | HCID 7187 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 12661867 | HCID 12661867 | — |
Reaction Steps
A mixture of 5-chloro-4-methyl-benzofuran with 5-chloro-6-methyl-benzofuran (19.6 g), N-bromosuccinimide (23 g) and benzoyl peroxide (160 mg) in carbon tetrachloride (350 ml) was heated under reflux under a 200 W lamp for 36 h. The cooled mixture was filtered through hyflo and the filtrate evaporated to give the title compound as a dark oil (28.8 g)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981572 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-459037a00a7146f485631410de6030c2 |
| Source note | uspto-grants-1999_11 |