HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10198333, compound → HCID 19611642, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10198333 | HCID 10198333 | — |
| Reactant | HCID 178418268 | HCID 178418268 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 19611642 | HCID 19611642 | 41.4% |
Reaction Steps
Lead tetraacetate (210 mg) was added to a solution of N-[3-(2,3-dihydro-benzofuran-4-yl)-propyl]-acetamide (100 mg) in acetic acid (1.5 ml) at 100. The mixture was stirred at room temperature for 2h and at 50° for 16 h. The solvent was evaporated and the residue purified by chromatography to give the title compound as an oil (41 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981572 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-5728706b3e8a45c19f8e43f00fcc82ec |
| Source note | uspto-grants-1999_11 |