HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 44214321, compound → HCID 44214325, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 44214321 | HCID 44214321 | — |
| Reactant | HCID 178418268 | HCID 178418268 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 44214325 | HCID 44214325 | 15.1% |
Reaction Steps
Lead tetraacetate (194 mg) was added to a solution of cyclopropanecarboxylic acid [3-(2,3-dihydro-benzofuran-4-yl)-propyl]-amide (100 mg) in acetic acid (1.5 ml) at 10°. The mixture was stirred at room temperature for 4 h and at 50° for 24 h. The solvent was evaporated and the residue purified by chromatography on silica. Elution with hexane/ethyl acetate gave the title compound as an oil (15 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981572 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-893ed6d228a449a3b4276cafe78b6e6d |
| Source note | uspto-grants-1999_11 |