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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1602424Generated: November 3, 2026

HCID 54171516, compound → HCID 54511393, compound

https://huagongshe.com/reaction/1602424

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54171516HCID 54171516—
SolventN,N-DiethylanilineHCID 7061—
ProductHCID 54511393HCID 545113933.9%

Reaction Steps

A solution of cyclopropanecarboxylic acid [3-(3-prop-2-ynyloxy-phenyl)-propyl]-amide (415 mg) in N,N-diethylaniline (2 ml) was heated at 215° C. for 24 h. The cooled mixture was purified by column chromatography on silica. Elution with hexane/ethyl acetate 3:1 gave the title compound (A) as a colourless solid (16 mg)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05981572
Source datasetuspto-grants-1999_11
ORD IDord-9912b5983d794e3288a205879f79c1f1
Source noteuspto-grants-1999_11