HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54171516, compound → HCID 54511393, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54171516 | HCID 54171516 | — |
| Solvent | N,N-Diethylaniline | HCID 7061 | — |
| Product | HCID 54511393 | HCID 54511393 | 3.9% |
Reaction Steps
A solution of cyclopropanecarboxylic acid [3-(3-prop-2-ynyloxy-phenyl)-propyl]-amide (415 mg) in N,N-diethylaniline (2 ml) was heated at 215° C. for 24 h. The cooled mixture was purified by column chromatography on silica. Elution with hexane/ethyl acetate 3:1 gave the title compound (A) as a colourless solid (16 mg)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981572 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-9912b5983d794e3288a205879f79c1f1 |
| Source note | uspto-grants-1999_11 |