HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53924084, compound → HCID 44214326, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53924084 | HCID 53924084 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 44214326 | HCID 44214326 | 73.1% |
Reaction Steps
A solution of cyclopropanecarboxylic acid [3-(2H-chromen-5-yl)-propyl]-amide (76 mg) in ethanol (5 ml) was hydrogenated over platinum (5% on carbon, 10 mg) for 16 h. The catalyst was filtered off and the filtrate evaporated. The residue was purified by column chromatography on silica. Elution with hexane/ethyl acetate 2:1 gave the title compound as a colourless solid (56 mg)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981572 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-9c070c2c090f4f2c824667b652ebb020 |
| Source note | uspto-grants-1999_11 |