HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → HCID 13170313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 18787473 | HCID 18787473 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 13170313 | HCID 13170313 | 93.4% |
Reaction Steps
2-Methyl-benzofuran-4-methanol (3.34 g, 21 mmol) was oxidized using DMSO, oxalyl chloride, and triethyl amine similar to the above procedures to give the product as a clear oil (3.14 g, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981571 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-f9e53cc3add744f483ee9c71a5a728a9 |
| Source note | uspto-grants-1999_11 |