HRID1602557

反应详情

EQUATION

反应方程式

HRID 1602557 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a suspension of norborn-5-en-2,3-dicarboxylic acid (5.01 g, 27.5 mmole) in H2O (50 mL) was added 1N aq. NaOH (55 mL, 55.0 mmol) at rt and the reaction mixture was stirred until a homogeneous solution was obtained. The solvent was removed in vacuo and the resulting colorless, crystalline product was dried: 5.57 g (90%), mp=385C.

WORKUP

后处理

  1. customwas obtained
  2. customThe solvent was removed in vacuo
  3. customthe resulting colorless, crystalline product was dried