Sodium Hydroxide → Sodium bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylate

Beteiligte Stoffe

Reaktionsschritte

To a suspension of norborn-5-en-2,3-dicarboxylic acid (5.01 g, 27.5 mmole) in H2O (50 mL) was added 1N aq. NaOH (55 mL, 55.0 mmol) at rt and the reaction mixture was stirred until a homogeneous solution was obtained. The solvent was removed in vacuo and the resulting colorless, crystalline product was dried: 5.57 g (90%), mp=385C.

Herkunft & Nachweise