Sodium Hydroxide → Sodium bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylate

Beteiligte Stoffe

Reaktionsschritte

To a suspension of bicyclo[2.2.2]-oct-5-en-2,3-dicarboxylic anhydride (2.01 g, 11.3 mmole) in MeOH (50 mL) was added 1 N aq. NaOH (22.4 mL, 22.4 mmol). The reaction mixture was stirred for 1 hour at room temperature. The solvent was removed in vacuo and the resulting colorless solid was dried: mp>400 C.

Herkunft & Nachweise