HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 53685075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 19612291 | HCID 19612291 | — |
| Reactant | HCID 178503020 | HCID 178503020 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53685075 | HCID 53685075 | — |
Reaction Steps
A solution of 30% sodium methoxide in methanol (0.3 ml, 1.6 mmol) is added over 8 hours to a mixture of methyl 3-[4-(1-adamantyl)-3-methoxybenzoylmethyloxy]-4-iodobenzoate (870 mg, 1.55 mmol) and methyltriphenylphosphine bromide (790 mg, 2.21 mmol) in THF (10 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981776 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-f48dfdf38f1a4ade8c6d7d8163dba406 |
| Source note | uspto-grants-1999_11 |