HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxymethylpyridine → HCID 15462314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxymethylpyridine | HCID 11472 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 19608373 | HCID 19608373 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15462314 | HCID 15462314 | — |
Reaction Steps
The procedure of Example 1 was followed except using 340 mg of 4-(hydroxymethyl)pyridine, 280 mg of 5-(3-acetoxybutyl)-7-chloropyrazolo[1,5-a]pyrimidine and 105 mg of 60% sodium hydride and using DMF as a solvent. The title compound was obtained as colorless crystals (50 mg). The structure and melting point of the compound obtained are shown in Table 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05985882 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-74119cc160b94115a58105b661a2f231 |
| Source note | uspto-grants-1999_11 |