HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15289126, compound → HCID 15289127, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15289126 | HCID 15289126 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15289127 | HCID 15289127 | — |
Reaction Steps
8.3 g (32.6 mmol) of 1-amino-4-benzyl-4-azatricyclo[5.2.2.02,6 ]undec-8-ene are hydrogenated in 100 ml of ethanol over 1 g of palladium/active charcoal at 100° C./100 bar. The catalyst is filtered off with suction, the filtrate is concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05986105 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-875da268b75e4473bba70763d2a28d10 |
| Source note | uspto-grants-1999_11 |