Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 1-Octene | HCID 8125 | — |
| Reactant | Triethoxysilane | HCID 13830 | — |
| Catalyst | Chloroplatinic acid | HCID 61859 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | Octyltriethoxysilane | HCID 76262 | 91% |
Reaction Steps
224 mg Of octene-1, 328 mg of triethoxysilane and 56 mg of toluene were placed in a glass reaction tube and 8 mg of benzoic acid added. Then, 0.001 ml of an isopropyl alcohol solution of chloroplatinic acid (platinum content: 0.39%) was added to this mixture. The reaction tube was sealed with Teflon tape and heated for 30 minutes in an oil bath at 50° C. When the contents were analyzed by GC-MS following cooling, the conversion rate of octene-1 was 97.5% and n-octyltriethoxysilane was produced at a yield of 91%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05986124 |
|---|
| Source dataset | uspto-grants-1999_11 |
|---|
| ORD ID | ord-a0799c6b8b3746a09ccb4dace06d22e6 |
|---|
| Source note | uspto-grants-1999_11 |
|---|
