HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 14358601, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 3-Methoxyphthalic acid | HCID 315218 | — |
| Catalyst | Cuprous chloride | HCID 62652 | — |
| Solvent | Methanol--water (1/1) | HCID 22242641 | — |
| Product | HCID 14358601 | HCID 14358601 | 63% |
Reaction Steps
A solution of methoxyphthalic acid obtained as per Example 5 (0.1 mol) in 100 ml methanol was added with CuCl (0.1 mol) and HCl (0.1 mol). The solution was heated to reflux for 30 min. The clear solution obtained was evaporated to dryness under reduced pressure. The residue obtained was dissolved in a 1:3 water-methanol mixture and acidified. The product was separated by cooling, collected by filtration and air dried. The product yield was 63-66%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05986129 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-a1929e08259e417fab59255c4b625ba9 |
| Source note | uspto-grants-1999_11 |