Diphenylamine → HCID 131721456, compound

HRID 1603290Notes

Reaction equation

HRID 1603290 reaction equation
[C:1]1([NH:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:14]=[CH:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>>[CH2:14]([C:12]1[C:13]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])=[C:8]([NH:7][C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[CH:9]=[CH:10][CH:11]=1)[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]

Participants

3

Reactant 2

HCID 11487DiphenylamineHCID 312851-Nonene

Product 1

HCID 131721456HCID 131721456, compoundYield 71%

Procedure

A commercial nonene yielded 59% dialkylate when reacted for 10 hours with diphenylamine under the conditions of Example 1. The nonene, after passing in the vapor phase over a 75 cc catalyst bed of F-24 at 650° F. for 5 seconds, was converted to a high reactivity alkene which yielded 71% dinonyl diphenylamine under the reaction conditions of Example 1 after 10 hours reaction time.

Sources & evidence

ORD record
ord-0d41e20a8a9e4fe6a37bc62dd32dfdb5
Source dataset
uspto-grants-1999_11
Patent number
US05986155

Reaction notes

Loading…