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HRID1603494

反应详情

EQUATION

反应方程式

HRID 1603494 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)c1ccccc1Br
HCID75060

2'-Bromoacetophenone

C8H7BrO

结构：CC(C)(C)OC(=O)NCC(N)=S
HCID5324304

tert-Butyl (2-amino-2-sulfanylideneethyl)carbamate

C7H14N2O2S

PRODUCTS

生成物

1
结构：c1ccc(-c2csc3cncn23)cc1
HCID23449301

未命名化合物

收率 66%

PROCEDURE

实验过程

The same procedure as in Preparation 10 was repeated except that 1.9 g of (N-t-butoxycarbonylamino) acetothioamide and 2.49 g of 2'-bromoacetophenone were used, thereby obtaining 1.32 g of the title compound.

WORKUP

后处理

  1. customThe same procedure as in Preparation 10