HuagongsheHuagongshe Chemistry Print Report · For research reference only
2'-Bromoacetophenone → 3-Phenylimidazo[5,1-b]thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2'-Bromoacetophenone | HCID 75060 | — |
| Reactant | tert-butyl N-(carbamothioylmethyl)carbamate | HCID 5324304 | — |
| Product | 3-Phenylimidazo[5,1-b]thiazole | HCID 23449301 | 66% |
Reaction Steps
The same procedure as in Preparation 10 was repeated except that 1.9 g of (N-t-butoxycarbonylamino) acetothioamide and 2.49 g of 2'-bromoacetophenone were used, thereby obtaining 1.32 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990101 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-3f00dd7ac2f5416d86580babc3c1595f |
| Source note | uspto-grants-1999_11 |