HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19605067, compound → HCID 19605222, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19605067 | HCID 19605067 | — |
| Reactant | Ammonia methanol | HCID 21705897 | — |
| Product | HCID 19605222 | HCID 19605222 | — |
Reaction Steps
A 294 mg potion of 2-ethoxycarbonylimidazo[5,1-b]thiazole was dissolved in 8 ml of a 2M ammonia/methanol solution, and the mixture was then stirred at room temperature for 4 days. After concentration under reduced pressure, 3 ml of dichloromethane was added to the resulting residue, and the precipitate was collected by filtration, washed with dichloromethane, and then dried under reduced pressure to obtain 226 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990101 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-5aec2c9db16642699d99be4294006eed |
| Source note | uspto-grants-1999_11 |