HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-[2-(2,5-Dimethoxyphenyl)ethenyl]-2-acetylamino benzoic acid methylester → HCID 54506424, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-[2-(2,5-Dimethoxyphenyl)ethenyl]-2-acetylamino benzoic acid methylester | HCID 54319513 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 54506424 | HCID 54506424 | — |
Reaction Steps
150 mg of 5-[2-(2,5-dimethoxyphenyl)ethenyl]-2-acetylamino benzoic acid methylester are dissolved in 10 ml of ethyl acetate. After addition of 25 mg of palladium (10% on charcoal) the mixture is stirred overnight under an atmosphere of hydrogen and filtered over celite. The filtrate is evaporated in vacuo to obtain the title compound as colourless crystals. mp:81-83°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990116 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-e04b782641e346d696ddb461e4e59762 |
| Source note | uspto-grants-1999_11 |